D a t a   F i l e   C : \ C H E M 3 2 \ 1 \ D A T A \ 1 5 0 9 2 2 _ S O L I D A G O _ S T A N D A R D S \ D E F _ L C   2 0 1 5 - 0 9 - 2 2   1 6 - 1 7 - 5 2 \ R U T I N _ 2 . D 
 
 S a m p l e   N a m e :   R u t i n _ 2 
 
 I n s t r u m e n t   1   9 / 2 3 / 2 0 1 5   1 : 2 3 : 5 8   A M   A K 
 
 
 
 = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = 
 
 A c q .   O p e r a t o r       :   A K                                                           S e q .   L i n e   :     1 0 
 
 A c q .   I n s t r u m e n t   :   I n s t r u m e n t   1                                         L o c a t i o n   :   V i a l   9 
 
 I n j e c t i o n   D a t e     :   9 / 2 3 / 2 0 1 5   1 2 : 4 3 : 3 0   A M                                 I n j   :       1 
 
                                                                                                 I n j   V o l u m e   :   1 5 . 0    l 
 
 S e q u e n c e   F i l e       :   C : \ C h e m 3 2 \ 1 \ D A T A \ 1 5 0 9 2 2 _ S o l i d a g o _ s t a n d a r d s \ D E F _ L C   2 0 1 5 - 0 9 - 2 2   1 6 - 1 7 - 5 2 \ D E F _ 
 
                                     L C . S 
 
 M e t h o d                     :   C : \ C H E M 3 2 \ 1 \ D A T A \ 1 5 0 9 2 2 _ S O L I D A G O _ S T A N D A R D S \ D E F _ L C   2 0 1 5 - 0 9 - 2 2   1 6 - 1 7 - 5 2 \ 
 
                                     R A Y K O D T A . M   ( S e q u e n c e   M e t h o d ) 
 
 L a s t   c h a n g e d         :   1 2 / 1 1 / 2 0 1 4   1 : 5 2 : 1 6   P M   b y   K S 
 
 M e t h o d   I n f o           :   S o l i d a g o   p h e n o l i c s   a n d   d i t e r p e n e   a c i d   a n a l y s i s 
 
 
 
 = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = 
 
                                                   A r e a   P e r c e n t   R e p o r t                                                   
 
 = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = 
 
 
 
 S o r t e d   B y                           :             S i g n a l 
 
 M u l t i p l i e r :                                       :             1 . 0 0 0 0 
 
 D i l u t i o n :                                           :             1 . 0 0 0 0 
 
 U s e   M u l t i p l i e r   &   D i l u t i o n   F a c t o r   w i t h   I S T D s 
 
 
 
 
 
 S i g n a l   1 :   D A D 1   A ,   S i g = 2 5 4 , 8   R e f = o f f 
 
 
 
 P e a k   R e t T i m e   T y p e     W i d t h           A r e a             H e i g h t           A r e a     
 
     #       [ m i n ]                 [ m i n ]       [ m A U * s ]           [ m A U ]                 % 
 
 - - - - | - - - - - - - | - - - - | - - - - - - - | - - - - - - - - - - | - - - - - - - - - - | - - - - - - - - | 
 
       1       1 . 4 4 2   B V         0 . 4 6 7 1     8 3 1 . 1 8 5 9 7       2 2 . 4 9 6 2 3       4 . 4 0 4 7 
 
       2       2 . 3 4 8   B V         0 . 1 9 0 1     4 9 6 . 1 2 7 5 3       3 7 . 5 5 1 5 2       2 . 6 2 9 1 
 
       3       2 . 6 9 2   V V         0 . 1 6 4 6     8 1 8 . 4 3 8 3 5       6 5 . 1 4 3 2 2       4 . 3 3 7 1 
 
       4       2 . 9 1 9   V V         0 . 2 5 3 4   2 2 3 4 . 7 2 3 3 9     1 1 8 . 8 3 5 7 2     1 1 . 8 4 2 4 
 
       5       3 . 6 9 4   V V         0 . 4 6 8 9   2 4 2 4 . 6 4 1 3 6       6 1 . 3 7 7 4 7     1 2 . 8 4 8 8 
 
       6       4 . 3 8 7   V V         0 . 5 2 4 6   2 2 2 3 . 2 7 7 1 0       5 4 . 2 0 0 4 8     1 1 . 7 8 1 7 
 
       7       4 . 8 1 7   V V         0 . 6 3 8 6   2 5 4 7 . 1 3 4 7 7       4 9 . 1 5 0 8 4     1 3 . 4 9 7 9 
 
       8       5 . 9 1 1   V B         0 . 6 7 1 0   1 9 6 8 . 5 0 9 0 3       3 8 . 0 8 6 5 7     1 0 . 4 3 1 6 
 
       9       6 . 6 9 8   B B         0 . 5 5 3 9   1 2 3 0 . 2 7 0 5 1       2 7 . 7 1 2 2 8       6 . 5 1 9 5 
 
     1 0       7 . 9 9 3   B B         0 . 3 6 6 6   2 1 3 0 . 0 7 4 7 1       8 0 . 0 1 4 0 2     1 1 . 2 8 7 8 
 
     1 1     1 0 . 9 2 5   B V         0 . 1 4 3 8       1 2 . 9 5 2 4 6         1 . 3 5 2 0 7       0 . 0 6 8 6 
 
     1 2     1 1 . 1 5 9   V B         0 . 1 7 1 1       2 8 . 3 6 9 2 2         2 . 3 4 6 0 6       0 . 1 5 0 3 
 
     1 3     1 4 . 1 0 2   B V         0 . 3 7 3 7       1 9 . 5 4 5 9 1   6 . 4 8 4 4 6 e - 1       0 . 1 0 3 6 
 
     1 4     1 5 . 1 8 4   V V         0 . 4 7 7 3       3 1 . 4 5 5 1 0   8 . 6 6 9 4 0 e - 1       0 . 1 6 6 7 
 
     1 5     1 6 . 3 7 8   V V         0 . 3 1 1 5       1 6 . 5 5 0 0 1   7 . 1 1 2 3 7 e - 1       0 . 0 8 7 7 
 
     1 6     1 6 . 9 0 9   V V         0 . 2 2 4 5         9 . 7 0 2 3 4   6 . 9 6 5 6 1 e - 1       0 . 0 5 1 4 
 
     1 7     1 7 . 2 9 5   V B         0 . 4 1 8 5       2 1 . 6 6 8 4 9   6 . 6 4 3 6 1 e - 1       0 . 1 1 4 8 
 
     1 8     1 8 . 3 6 7   B V         0 . 2 7 1 0       1 6 . 5 2 6 0 7   9 . 3 1 3 8 1 e - 1       0 . 0 8 7 6 
 
     1 9     1 8 . 9 8 8   V V         0 . 8 4 6 1       6 7 . 7 1 4 8 6   9 . 9 9 8 4 7 e - 1       0 . 3 5 8 8 
 
     2 0     2 1 . 7 3 1   V V         0 . 3 4 4 6       2 5 . 8 8 4 2 2   9 . 6 5 9 7 3 e - 1       0 . 1 3 7 2 
 
     2 1     2 5 . 7 7 1   V V         0 . 2 1 2 2       1 0 . 4 0 7 3 7   6 . 8 8 9 0 8 e - 1       0 . 0 5 5 2 
 
     2 2     2 6 . 4 7 9   V V         0 . 3 0 6 5       2 2 . 9 0 1 7 6   9 . 4 5 9 2 0 e - 1       0 . 1 2 1 4 
 
     2 3     2 6 . 9 7 4   V V         0 . 3 2 5 4       3 1 . 0 1 9 1 2         1 . 2 1 6 8 6       0 . 1 6 4 4 
 
     2 4     2 7 . 3 7 3   V V         0 . 2 5 1 4       1 9 . 9 1 1 7 6         1 . 0 5 8 6 4       0 . 1 0 5 5 
 
     2 5     2 8 . 0 3 1   V V         0 . 3 2 3 7       2 6 . 8 3 4 4 6         1 . 0 4 4 6 4       0 . 1 4 2 2 
 
     2 6     3 4 . 4 0 1   V B A       0 . 2 6 3 1   1 6 0 4 . 7 6 5 3 8       7 8 . 3 0 7 9 1       8 . 5 0 4 1 
 
 T o t a l s   :                                     1 . 8 8 7 0 6 e 4       6 4 8 . 0 1 4 1 1 
 
 
 
 
 
 S i g n a l   2 :   D A D 1   C ,   S i g = 3 2 0 , 8   R e f = o f f 
 
 
 
 P e a k   R e t T i m e   T y p e     W i d t h           A r e a             H e i g h t           A r e a     
 
     #       [ m i n ]                 [ m i n ]       [ m A U * s ]           [ m A U ]                 % 
 
 - - - - | - - - - - - - | - - - - | - - - - - - - | - - - - - - - - - - | - - - - - - - - - - | - - - - - - - - | 
 
       1       2 . 3 4 5   B V         0 . 1 5 6 0     1 9 1 . 3 2 6 3 9       1 8 . 5 9 7 2 8       2 . 3 1 8 6 
 
       2       2 . 6 8 9   V V         0 . 1 4 9 2     6 5 3 . 2 6 0 3 1       5 8 . 0 6 9 7 9       7 . 9 1 6 5 
 
       3       2 . 9 1 5   V V         0 . 2 4 9 8   2 1 5 2 . 0 9 7 6 6     1 1 5 . 2 7 3 9 2     2 6 . 0 8 0 0 
 
       4       4 . 3 9 2   V V         1 . 3 2 9 1   3 6 4 0 . 5 6 2 2 6       3 3 . 1 0 0 9 4     4 4 . 1 1 7 8 
 
       5       7 . 9 9 2   B B         0 . 2 6 2 7     6 3 5 . 7 4 2 6 1       3 5 . 8 8 9 3 1       7 . 7 0 4 2 
 
       6     1 1 . 1 5 9   V B         0 . 1 4 5 0       1 1 . 6 9 6 1 2         1 . 2 0 7 9 6       0 . 1 4 1 7 
 
       7     2 6 . 9 6 9   V V         0 . 7 0 0 6       6 6 . 9 4 8 8 5         1 . 1 7 1 7 0       0 . 8 1 1 3 
 
       8     2 8 . 0 2 3   V V         0 . 3 3 3 7       2 6 . 0 6 2 1 8         1 . 0 0 1 2 8       0 . 3 1 5 8 
 
       9     3 0 . 4 0 1   B V         0 . 3 9 5 9       3 8 . 1 1 8 3 7         1 . 2 2 2 1 5       0 . 4 6 1 9 
 
     1 0     3 4 . 7 0 0   V B A       1 . 8 8 6 3     8 3 6 . 0 9 8 0 2         5 . 2 3 7 8 3     1 0 . 1 3 2 2 
 
 T o t a l s   :                                     8 2 5 1 . 9 1 2 7 7     2 7 0 . 7 7 2 1 6 
 
 
 
 
 
 S i g n a l   3 :   D A D 1   D ,   S i g = 3 6 0 , 8   R e f = o f f 
 
 
 
 P e a k   R e t T i m e   T y p e     W i d t h           A r e a             H e i g h t           A r e a     
 
     #       [ m i n ]                 [ m i n ]       [ m A U * s ]           [ m A U ]                 % 
 
 - - - - | - - - - - - - | - - - - | - - - - - - - | - - - - - - - - - - | - - - - - - - - - - | - - - - - - - - | 
 
       1       1 . 4 5 1   B V         0 . 3 8 1 1     7 0 6 . 6 3 2 8 7       2 2 . 4 5 8 6 4       7 . 0 5 0 9 
 
       2       2 . 3 4 6   B V         0 . 1 7 0 7     4 3 4 . 7 2 2 9 9       3 7 . 6 6 0 1 5       4 . 3 3 7 7 
 
       3       2 . 6 8 8   V V         0 . 1 6 1 0     8 3 0 . 0 0 4 6 4       6 7 . 7 0 7 7 6       8 . 2 8 1 9 
 
       4       2 . 9 1 4   V V         0 . 2 5 0 3   2 2 8 2 . 0 3 0 7 6     1 2 1 . 9 8 6 4 1     2 2 . 7 7 0 5 
 
       5       3 . 7 3 9   V V         0 . 4 8 2 9   2 0 6 5 . 0 3 4 4 2       5 1 . 6 0 0 2 4     2 0 . 6 0 5 3 
 
       6       4 . 3 8 6   V V         0 . 5 9 6 3   1 5 6 4 . 7 6 3 0 6       3 2 . 6 9 6 1 6     1 5 . 6 1 3 5 
 
       7       7 . 9 9 3   B B         0 . 2 6 5 5   1 0 4 8 . 6 0 6 5 7       5 8 . 4 0 3 2 7     1 0 . 4 6 3 2 
 
       8     1 0 . 9 2 9   B V         0 . 1 4 0 4       1 2 . 2 4 9 9 2         1 . 3 1 8 8 2       0 . 1 2 2 2 
 
       9     1 1 . 1 6 0   V B         0 . 1 4 7 3       1 9 . 3 6 9 2 3         1 . 9 2 6 2 1       0 . 1 9 3 3 
 
     1 0     1 2 . 0 5 7   B B         0 . 3 3 3 3         8 . 6 0 3 7 6   3 . 3 5 4 1 1 e - 1       0 . 0 8 5 8 
 
     1 1     1 4 . 1 0 6   B B         0 . 3 8 3 3       1 9 . 6 9 7 0 0   6 . 3 6 0 6 4 e - 1       0 . 1 9 6 5 
 
     1 2     1 5 . 1 8 5   B B         0 . 2 9 6 8       1 5 . 2 3 8 8 2   6 . 8 7 0 6 9 e - 1       0 . 1 5 2 1 
 
     1 3     1 6 . 9 1 9   B V         0 . 1 4 8 8         5 . 2 5 3 4 7   4 . 9 1 0 9 0 e - 1       0 . 0 5 2 4 
 
     1 4     1 7 . 3 0 7   V B         0 . 1 4 4 7         4 . 9 3 8 4 7   4 . 3 4 2 1 3 e - 1       0 . 0 4 9 3 
 
     1 5     2 0 . 9 9 1   B V         0 . 2 9 9 7       1 4 . 4 0 3 1 4   6 . 1 8 5 5 6 e - 1       0 . 1 4 3 7 
 
     1 6     2 1 . 7 2 1   V B         0 . 3 0 9 1       1 8 . 6 4 3 3 4   8 . 0 2 3 2 2 e - 1       0 . 1 8 6 0 
 
     1 7     2 4 . 7 2 9   B V         0 . 1 7 0 7         4 . 4 2 2 2 8   4 . 2 0 3 2 2 e - 1       0 . 0 4 4 1 
 
     1 8     2 5 . 1 6 9   V B         0 . 2 0 0 2         8 . 3 6 7 7 7   5 . 3 5 7 0 9 e - 1       0 . 0 8 3 5 
 
     1 9     2 5 . 7 5 0   B V         0 . 2 1 2 9       1 0 . 7 3 3 5 4   6 . 7 0 0 3 1 e - 1       0 . 1 0 7 1 
 
     2 0     2 6 . 9 6 5   V V         0 . 6 8 8 0       6 8 . 9 4 6 6 4         1 . 2 0 7 7 4       0 . 6 8 8 0 
 
     2 1     2 8 . 0 1 8   V V         0 . 3 6 3 1       2 9 . 3 8 4 2 5         1 . 0 1 0 8 2       0 . 2 9 3 2 
 
     2 2     2 9 . 0 4 2   V V         0 . 4 5 9 6       2 5 . 9 6 6 1 9   6 . 9 5 4 9 0 e - 1       0 . 2 5 9 1 
 
     2 3     3 0 . 4 0 5   B V         0 . 4 3 8 4       5 1 . 9 4 6 5 6         1 . 4 5 5 4 6       0 . 5 1 8 3 
 
     2 4     3 3 . 8 9 0   V V         1 . 5 5 7 8     6 0 7 . 9 4 1 6 5         4 . 6 3 0 2 6       6 . 0 6 6 2 
 
     2 5     3 4 . 6 8 0   V B A       0 . 4 3 6 9     1 6 3 . 9 6 4 1 1         4 . 5 2 2 8 4       1 . 6 3 6 1 
 
 T o t a l s   :                                     1 . 0 0 2 1 9 e 4       4 1 4 . 9 1 1 0 7 
 
 
 
 
 
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 
 
 
 P e a k   R e t T i m e   T y p e     W i d t h           A r e a             H e i g h t           A r e a     
 
     #       [ m i n ]                 [ m i n ]       [ m A U * s ]           [ m A U ]                 % 
 
 - - - - | - - - - - - - | - - - - | - - - - - - - | - - - - - - - - - - | - - - - - - - - - - | - - - - - - - - | 
 
       1       2 . 5 0 7   B V         0 . 2 3 6 0   1 0 4 1 . 1 4 4 9 0       6 7 . 4 7 2 8 8       2 . 4 9 7 0 
 
       2       2 . 9 5 2   V V         0 . 1 3 5 8     6 9 9 . 8 5 5 5 3       7 5 . 7 1 1 6 5       1 . 6 7 8 5 
 
       3       3 . 1 1 9   V V         0 . 1 0 1 9     8 4 3 . 1 9 8 6 1     1 2 0 . 1 5 5 7 1       2 . 0 2 2 3 
 
       4       3 . 3 6 2   V V         0 . 6 0 2 1   2 1 8 1 . 5 2 9 3 0       4 6 . 9 4 8 4 9       5 . 2 3 2 0 
 
       5       4 . 3 7 0   V B         0 . 3 6 9 0     5 7 4 . 2 1 9 6 0       2 0 . 6 1 0 5 3       1 . 3 7 7 2 
 
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 
       7       7 . 9 9 3   V B         0 . 2 7 1 4   2 1 7 0 . 1 3 0 8 6     1 1 9 . 7 8 3 1 4       5 . 2 0 4 7 
 
       8     1 0 . 9 3 4   B V         0 . 5 5 6 9     2 3 8 . 9 6 4 6 9         5 . 3 1 0 9 4       0 . 5 7 3 1 
 
       9     1 1 . 1 6 1   V B         0 . 3 5 5 4     1 9 4 . 9 6 9 8 3         6 . 9 4 6 6 0       0 . 4 6 7 6 
 
     1 0     1 3 . 3 5 9   B V         0 . 9 8 0 3     5 4 5 . 5 2 3 6 2         6 . 6 8 2 8 8       1 . 3 0 8 3 
 
     1 1     1 6 . 9 3 8   V V         2 . 0 7 1 1   2 0 3 2 . 1 2 6 2 2       1 1 . 6 2 6 5 8       4 . 8 7 3 7 
 
     1 2     1 7 . 3 1 2   V V         0 . 3 5 8 3     3 5 1 . 5 4 1 9 0       1 2 . 1 2 2 3 7       0 . 8 4 3 1 
 
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 
     1 4     1 9 . 0 1 7   V V         0 . 4 3 5 2     4 6 4 . 6 6 1 9 9       1 3 . 3 1 3 3 0       1 . 1 1 4 4 
 
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 
     1 6     2 0 . 8 7 0   V V         0 . 9 0 8 9   1 1 1 2 . 7 7 8 2 0       1 4 . 8 7 2 2 5       2 . 6 6 8 8 
 
     1 7     2 1 . 7 4 0   V B         0 . 7 0 2 8     8 6 6 . 0 6 0 7 9       1 5 . 2 4 5 6 0       2 . 0 7 7 1 
 
     1 8     2 2 . 8 7 5   B V         0 . 4 8 3 1     6 8 8 . 0 2 5 1 5       1 7 . 6 3 7 4 9       1 . 6 5 0 1 
 
     1 9     2 3 . 3 4 6   V B         0 . 3 7 9 6     5 1 5 . 9 3 6 3 4       1 7 . 3 1 4 9 0       1 . 2 3 7 4 
 
     2 0     2 4 . 1 1 2   B V         0 . 6 1 7 0     8 6 5 . 8 0 1 6 4       1 7 . 6 2 9 2 1       2 . 0 7 6 5 
 
     2 1     2 4 . 7 6 0   V V         0 . 2 8 0 5     3 5 9 . 9 4 1 3 5       1 7 . 7 5 9 1 6       0 . 8 6 3 3 
 
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 
     2 3     2 5 . 9 7 0   V V         0 . 4 5 8 7     7 6 7 . 5 2 4 1 7       2 0 . 4 1 3 5 3       1 . 8 4 0 8 
 
     2 4     2 6 . 2 7 6   V V         0 . 2 1 1 4     3 0 4 . 9 5 8 1 6       2 0 . 2 8 4 9 5       0 . 7 3 1 4 
 
     2 5     2 7 . 4 1 5   V V         0 . 9 4 8 2   1 6 7 3 . 5 1 2 3 3       2 2 . 0 8 2 3 2       4 . 0 1 3 6 
 
     2 6     2 8 . 1 2 1   V V         0 . 4 1 1 3     7 2 6 . 1 7 3 4 0       2 2 . 5 7 6 3 8       1 . 7 4 1 6 
 
     2 7     2 9 . 0 7 0   V V         0 . 6 6 7 6   1 3 0 2 . 5 6 5 6 7       2 3 . 7 5 8 6 4       3 . 1 2 4 0 
 
     2 8     3 4 . 4 0 0   V B A       0 . 3 4 1 2   1 . 9 0 0 2 5 e 4       6 9 8 . 8 3 4 0 5     4 5 . 5 7 4 3 
 
 T o t a l s   :                                     4 . 1 6 9 5 6 e 4     1 4 6 3 . 7 6 3 8 6 
 
 
 
 
 
 S i g n a l   5 :   D A D 1   B ,   S i g = 2 3 0 , 8   R e f = o f f 
 
 
 
 P e a k   R e t T i m e   T y p e     W i d t h           A r e a             H e i g h t           A r e a     
 
     #       [ m i n ]                 [ m i n ]       [ m A U * s ]           [ m A U ]                 % 
 
 - - - - | - - - - - - - | - - - - | - - - - - - - | - - - - - - - - - - | - - - - - - - - - - | - - - - - - - - | 
 
       1       2 . 3 7 2   B V         0 . 1 9 2 6     3 0 1 . 6 2 9 3 6       2 2 . 4 6 5 1 7       0 . 4 1 0 7 
 
       2       2 . 5 7 1   V V         0 . 2 0 4 8     5 7 4 . 2 5 6 7 1       4 1 . 6 7 1 5 6       0 . 7 8 1 9 
 
       3       2 . 9 2 9   V V         0 . 1 7 1 9   1 0 4 9 . 1 6 0 7 7       8 7 . 4 9 6 7 6       1 . 4 2 8 5 
 
       4       3 . 1 0 5   V V         0 . 1 0 2 1     5 8 8 . 9 8 0 1 6       8 8 . 0 2 2 6 8       0 . 8 0 1 9 
 
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 
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 
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 
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 
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 
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 
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 
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 
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 
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 
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 
     1 6     1 4 . 2 7 5   V V         0 . 9 7 1 4   2 9 6 1 . 6 7 1 3 9       3 6 . 9 3 8 7 1       4 . 0 3 2 6 
 
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 
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 
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 
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 
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 
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 
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 
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 
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 
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 
     2 7     2 4 . 3 6 5   V V         0 . 8 3 0 3   1 8 9 3 . 2 9 3 0 9       2 8 . 3 7 9 9 5       2 . 5 7 7 9 
 
     2 8     2 4 . 7 7 1   V V         0 . 2 6 6 5     5 5 4 . 3 3 2 8 2       2 8 . 0 5 6 1 7       0 . 7 5 4 8 
 
     2 9     2 5 . 2 1 5   V V         0 . 3 1 6 3     7 1 5 . 9 5 4 0 4       2 7 . 8 1 5 8 8       0 . 9 7 4 8 
 
     3 0     2 5 . 9 7 7   V V         0 . 5 3 5 1   1 2 1 5 . 7 2 7 4 2       2 8 . 1 9 0 3 3       1 . 6 5 5 3 
 
     3 1     2 7 . 4 2 9   V V         1 . 1 2 5 5   2 6 9 0 . 5 3 8 5 7       2 9 . 2 4 1 6 1       3 . 6 6 3 4 
 
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 
     3 3     3 4 . 4 0 0   V B A       0 . 5 3 8 0   2 . 0 4 4 6 6 e 4       4 6 4 . 0 8 0 1 4     2 7 . 8 3 9 8 
 
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 
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 
                                                     * * *   E n d   o f   R e p o r t   * * * 
 
 